Section
Introduction The purpose of this lab was to find the amount and percentage of nickel present in an unknown compound using the "mole method." The unknown nickel compound was dissolved in water and treated with dimethylglyoxime and ammonia solutions to obtain the precipitate of known chemical composition (bis(dimethylglyoximo)nickel(II)), which then was weighed and using this data the amount and percentage of nickel in the initial compound were found. The insoluble Ni(DMG)2 complex is formed in two steps. First, the dimethylglyoxime reacts with hydroxide ion formed through the ammonia hydrolysis to produce dimethylglyoximate anion: C4H8N2O2( ...
