Crystallization Reports Samples For Students

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Introduction and Literature Review

The value for a drug is significantly impacted by the dissolution rate, chemical stability and solubility of the drugs thereby impacting the pharmaceuticals efficiency as well. In the pharmaceutical industry multi-component crystals such as hydrates, solvates, co-crystals and salts have a major role during the design of new solids. Solid does not self-crystallize. It crystallizes in varied forms depicting random crystal properties. Various approaches are used to modify solids like Salting, Solvation, Hydration, and Polymorphism. Apart from these approaches, Co-Crystallization is a promising new approach to modifying solids (Nauha, ...

Abstract

In this experiment, 5 mL of toluene solution was transferred in a 25 mL round bottom flask and then 0.40 g maleic anhydride and 0.4 g E, E-2, 4-hexadien-1-l added. Ethyl acetate was used as a solvent to carry out a TLC analysis on the mixture produced after reaction completion mainly to determine the presence of any starting material in the mixture. The reaction mixture was then slowly cooled to room temperature. There was crystallization taking place as the reaction cooled, white crystals were formed.
The mixture was further cooled in for 10 minutes in a water bath to promote crystallization to ...

Research Question

The effect of increasing the concentration of two reactants, i.e. Calcium Chloride solution and Sodium Carbonate solution, on the percentage yield of Calcium Carbonate is to be studied in this experiment. The efficiency analysis for the production of Calcium Carbonate (also known as chalk) is to be carried out.
The dependent variable in this experiment is the percentage yield of Calcium Carbonate, expressed as percentage (%). The independent variable is the concentration of the reactants, i.e. Calcium Chloride solution and Sodium Carbonate solution. The concentrations are expressed in moles/liter or moles/dm3. While the control variable is the mass of the ...

Introduction

Extraction, crystallization and melting point can be used as methods of separating mixtures. Extraction and melting points are employed on separating liquid-liquid mixtures whereas purification of elements utilizes crystallization as their method of separation with impurities. Separation of mixtures involves the distinction of the constituent elements of the mixture into their constituent elements. Separation of mixtures is based on characteristics of the constituent elements of the mixture. Chemical affinity and density are the most utilized properties in organic compound mixtures.

Discussion

Methods of preparing the substance include the use of extraction from a mixture which is based on the principle of ...

Abstract

The experiment conducted is a palladium catalyzed coupling of a terminal alkyne to 4-Iodonitrobenzene. 1.25 mL of 95% ethanol was added along with 93mg of 4-Iodonitrobenzene, 80mg piperazine hexahydrate and 4 mg CuI, in a 5mL clean and dry conical vial plus spinvane. 80 µL (density 0.898 g/mL) of tetrahydro-2-(2-propynyloxy)-2H-pyran was added to the solution through an automatic pipette. To this add 3 mg of Pd(OAc)2, refluxed and stirred under a water cooled condenser for half an hour until it turned dark brown. The reaction mixture was then poured into a clean and dry evaporating dish and heated gently with a ...

Introduction

Aspirin is a commonly used drug. One of the properties of aspirin is that it is an analgesic, meaning that it relieves of pain. Aspirin is also an antipyretic drug meaning that it relieves on of fever. It also has anti-inflammatory properties meaning that if readily relieves swelling from tissues (Ahluwalia, Sunita & Adarsh 231). Salicylic acid has two functional groups. One of the functional groups is the phenolic group while the other functional group is carboxylic acid group. The presence of these two functional groups means that salicylic acid can undergo esterification in two different reactions.
In one reaction, ...